Metrohm 797 VA Computrace manuali

Metrohm 797 VA Computrace Manuale Utente (307 pagine)

Marchio: Metrohm | Categoria: Software | Dimensione: 3.25 MB |

Inglese

Tedesco

Indice

797 VA Computrace

1

Inhaltsverzeichnis

5

797 VA Computrace – Software

10

1 Einführung

13

1.2 Allgemeine Informationen

14

1.3 Installation

14

1.6 Kontext-sensitive Menüs

21

2 Hauptfenster

22

2.3 Menü «File»

25

2.4 Menü «Mode»

29

2.5 Menü «Utility»

29

2.6 Menü «User»

30

2.7 Menü «Settings»

34

2.8 Menü «Window»

48

ein-/ausschalten

50

«Exploratory» und «Determi

51

Drop size [ 1...9 ; 4 ]

52

3.2 VA-Messmodi

55

Square wave

57

Mode im Fenster EXPLORATORY

57

SPECIFICATION

57

Start potential

59

CV - Cyclic vol

63

CIFICATION

63

AC - Alternating current

69

3.3 Potentiostat

76

3.5 Grafische Einstellungen

80

4 Betriebsart «Exploratory»

86

4.3 Signalkurven

91

5.2 Arbeitsmethode

103

Conc. beziehen sich auf die

107

Cell no. X [ > 0 ; 0 ]

119

PARAMETERS

119

5.3 Monitor

124

CONFIRMATION

125

Data in memory

125

MONITOR

126

5.4 Bestimmungskurven

134

DETERMINATION CURVES

137

5.5 Resultate

146

Conc

148

Electrode test

150

5.6 Probentabelle

151

Conc. beziehen sich

152

Order [ 1...6 ; ]

155

Sample table

155

Voltammogramm

159

Chronoamperogramm

159

Conc.dev

165

Conc.± Conc.dev

165

6 Galvanikbad VA

167

Conc. bezie

203

Calibration-Techniken der

212

7 Handbedienung

216

7.2 Dosiergeräte-Steuerung

218

7.3 Pumpen-Steuerung

219

7.4 Filmbildung

221

7.5 Reinigung

222

8 Wie gehe ich vor ...?

225

8.2 Anwenderzugriffsrechte

226

Spüllösung

248

Intercept-Lösung

252

Suppressor-Standard

258

Calibration

264

Calibration-Technik "RC

265

8.8 Kalibrierkurven-Technik

272

8.10 Diagnose

277

9 Fehlerbehebung

281

9.4 Dosiergerät Probleme

282

DOSINO CONTROL

283

METHOD SPECIFICATION

285

9.6 Voltammetrische Probleme

286

Highest current range: 10 μA

289

Front end oder Rear end für

299

Softwarelizenzvereinbarung

301

Index

305

Metrohm 797 VA Computrace Manuale Utente (128 pagine)

Marchio: Metrohm | Categoria: Software | Dimensione: 3.22 MB |

Tedesco

Indice

797 VA Computrace

1

Inhaltsverzeichnis

5

Abbildungsverzeichnis

7

1 Einleitung

9

1.2 Bedienungselemente

10

Details siehe Kap

13

1.3.1 Aufbau

15

Parameter oder Eingabewert

16

1.4.1 Applikations-Bulletins

17

1 Einleitung

18

1.4.2 Application Notes

19

1.4.3 Monographien

19

1.4.4 Nachdrucke

19

2 Installation

20

2.2.3 Anschluss am PC

21

6.2151.020 USB-Kabel

22

43 (6.0343.000 Pt

24

2.2.5 Inertgas-Anschluss

25

2.3.3 Kapillare montieren

31

797 VA COMPUTRACE /

32

Utility / Computrace control

32

COMPUTRACE CONTROL zu

32

Ende die Schlauchkopplung

33

2.3.6 Aufbewahren der MME

37

2.3.8 Wechsel der Kapillare

38

2.3.9 Reinigung der MME

39

2.4.2 Regenerierung der RDE

42

2.5 Bezugselektrode

44

2.5.2 Inbetriebnahme

45

2.6 Hilfselektrode

46

2.7 Rührer

47

2.8.1 Elektrischer Anschluss

48

2.8.2 Schlauchanschluss

49

DOSINO CONTROL zu öffnen

50

DOSINO CONTROL schliessen

50

Empty via port muss

50

2.9.1 Elektrischer Anschluss

56

2.9.2 Schlauchverbindungen

58

2.9.3 Softwareeinstellungen

60

Automation

62

2.10.1 Allgemeiner Aufbau

65

0.5 ... 1 mm

66

800 Dosino

70

Probenvolumen > 10 mL

73

Probenvolumen <10 mL

74

Met roh m

76

2.11 Steuerungsleitungen

77

Measurement

79

Measure Intercept

81

2 Installation

82

RC Record response curve

83

RC Sample with response curve

84

3 Sicherheit

85

3.2 Sicherungen wechseln

86

3.3 Gehäusetemperatur

86

4 Anhang

91

Elektrodentips 6.1204.XXX

92

4.2 Lieferumfang

97

6.2709.040 Stopfen

106

4.3 Optionen

108

4.4 Validierung / GLP

121

4.5.1 Gewährleistung

122

(6.2141.170)

125

Ordering designation...111

125

4 Anhang

126

112 (6.0343.000)

127

Metrohm 797 VA Computrace Manuale Utente (127 pagine)

Marchio: Metrohm | Categoria: Software | Dimensione: 3.38 MB |

Inglese

Indice

797 VA Computrace

1

Table of contents

5

List of figures

7

1 Introduction

9

1.2 Parts and controls

10

1.3.1 Organization

15

Parameter or entry value

16

1.4 Support documentation

17

1.4.2 Application Notes

18

1.4.3 Monographs

19

1.4.4 Reprints

19

2 Installation

20

2.2.3 Connection to the PC

21

6.2151.020 USB Cable

22

2.2.5 Inert gas connection

25

MAIN WINDOW / Utility

32

/ Computrace control

32

DME in the COM

32

2.3.6 Storing the MME

37

2.3.8 Changing capillary

37

2.3.9 Cleaning the MME

39

2.4.2 Regeneration of RDE

42

2.5 Reference electrode

44

2.5.2 Startup procedure

45

2.6 Auxiliary electrode

46

2.7 Stirrer

47

2.8.1 Electrical connection

48

2.8.2 Tubing connection

48

DOSINO CONTROL window

50

2.9.1 Electrical connection

55

2.9.2 Tubing connections

56

2.9.3 Software settings

59

Automation tab

60

Relay box

60

2 Installation

62

2.10.1 General composition

63

0.5 ... 1 mm

64

800 Dosin o

65

800 Dosi no

65

800 Dosino

68

Sample volume > 10 mL

71

2.11 Control lines

75

Measurement

77

Timeline

78

Measure Intercept

79

RC Record response curve

81

3 Safety

83

3.2 Change fuses

84

3.3 Cabinet temperature

84

3.4.1 Properties of mercury

85

3.4.3 Handling of mercury

86

[16] Quecksilberreinigung

89

(1962), 351

89

4 Appendix

90

4.2 Scope of delivery

96

6.2709.040 Stopper

105

4.3 Options

107

4.3 Options

119

4.4 Validation / GLP

120

4.5.1 Warranty

121

4.6 Index

123

4 Appendix

124

4.6 Index

125

Metrohm 797 VA Computrace Manuale Utente (295 pagine)

Marchio: Metrohm | Categoria: Software | Dimensione: 3.15 MB |

Inglese

Indice

797 VA Computrace

1

Table of contents

10

Table of contents

11

1 Introduction

13

1.2 General information

14

1.3 Installation

14

1.3 Installation

15

1 Introduction

16

1.5 Overview of file types

19

1.6 Context sensitive menus

20

2 Main window

21

2 Main window

22

2.3 File menu

24

2.3 File menu

25

2.4 Mode menu

27

2.5 Utility menu

28

2.6 User menu

28

2.6 User menu

29

2.7 Settings menu

32

2.7 Settings menu

33

2.8 Window menu

46

2.8 Window menu

47

3.1 Electrodes

48

3.1 Electrodes

49

Drop size [ 1...9 ; 4 ]

50

3.2 VA measurement modes

52

3.2 VA measurement modes

53

METHOD SPECIFICATIONS

54

KING METHOD SPECIFICATIONS

56

Normal pulse

58

3.3 Potentiostat

71

3.5 Graphical settings

76

3.5 Graphical settings

77

Color of the line

81

4 Exploratory mode

82

4 Exploratory mode

84

4.3 Exploratory curves

86

4.3 Exploratory curves

87

PLORATORY CURVES

97

EXPLORA

97

TORY SPECIFICATION

97

5 Determination mode

98

5 Determination mode

100

797 VA Computrace – Software

101

5.3 Monitor

120

5.3 Monitor

121

5.4 Determination curves

130

5.4 Determination curves

131

5.5 Results

141

5.5 Results

143

Electrode test

145

5.6 Sample table

146

5.6 Sample table

147

Voltammogram

154

Chronoamperogram

154

Minimum

157

Recommended

157

6 Electroplating Bath VA

162

Calibra

205

Calibration

205

Calibration tech

207

7 Manual control

209

7 Manual control

210

7.2 Dosing Device control

211

7.3 Pump control

212

7.4 Film deposition

213

7.5 Cleaning procedure

215

8 How to ...?

217

8.2 User rights

218

DOSINOS window:

239

Suppressor standard

247

Rinsing solution

247

Response curve)

253

8.10 Diagnostic procedures

265

9 Troubleshooting

269

9.4 Dosing Device problems

270

9 Troubleshooting

272

AC – Alternating

273

FICATION

273

METHOD PARAMETERS

273

9.6 Voltammetric problems

274

9.6 Voltammetric problems

275

Software license

288

Software license

289

Index

291

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