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6 Electroplating Bath VA
797 VA Computrace – Software
150
6 Electroplating Bath VA
6.1 Electroplating Bath VA – Introduction
The 797 VA Computrace has two special modes for electroplating
bath analysis: CVS (Cyclic Voltammetric Stripping) and CPVS (Cy-
clic Pulse Voltammetric Stripping). Working with these two modes,
you have to consider that some settings and options differ from
working with the other modes.
6.2 Calibration techniques with CVS and CPVS
With CVS and CPVS, 8 Calibration techniques are available:
• Standard addition plating bath
• LAT Record intercept value
• LAT Standard addition for brighteners
• MLAT Standard addition for brighteners
• DT Suppressors with calibration curve
• DT Record calibration curve
• RC Sample with response curve
• RC Record response curve
Standard addition plating bath
“Standard addition plating bath” is a
Calibration technique for CVS
and CPVS. It is mainly used to develop methods:
• Optimize addition volumes and concentrations (e.g. to get
“Addition ratio” after 5 to 20 additions for “DT Record cali-
bration curve” and “DT Suppressors with calibration curve”)
• Optimize dilution with "Intercept solution" for “MLAT”
• Check linear range of standard addition (with “LAT” and
“MLAT”)
Determination tab with Calibration technique “Standard
addition plating bath”
The
Determination tab of the EDIT WORKING METHOD PARAME-
TERS
window contains general specifications for performing the
- 797 VA Computrace 1
- Table of contents 10
- Table of contents 11
- 1 Introduction 13
- 1.2 General information 14
- 1.3 Installation 14
- 1.3 Installation 15
- 1 Introduction 16
- 1.5 Overview of file types 19
- 1.6 Context sensitive menus 20
- 2 Main window 21
- 2 Main window 22
- 2.3 File menu 24
- 2.3 File menu 25
- 2.4 Mode menu 27
- 2.5 Utility menu 28
- 2.6 User menu 28
- 2.6 User menu 29
- 2.7 Settings menu 32
- 2.7 Settings menu 33
- 2.8 Window menu 46
- 2.8 Window menu 47
- 3.1 Electrodes 48
- 3.1 Electrodes 49
- Drop size [ 1...9 ; 4 ] 50
- 3.2 VA measurement modes 52
- 3.2 VA measurement modes 53
- METHOD SPECIFICATIONS 54
- KING METHOD SPECIFICATIONS 56
- Normal pulse 58
- 3.3 Potentiostat 71
- 3.5 Graphical settings 76
- 3.5 Graphical settings 77
- Color of the line 81
- 4 Exploratory mode 82
- 4 Exploratory mode 84
- 4.3 Exploratory curves 86
- 4.3 Exploratory curves 87
- PLORATORY CURVES 97
- EXPLORA 97
- TORY SPECIFICATION 97
- 5 Determination mode 98
- 5 Determination mode 100
- 797 VA Computrace – Software 101
- 5.3 Monitor 120
- 5.3 Monitor 121
- 5.4 Determination curves 130
- 5.4 Determination curves 131
- 5.5 Results 141
- 5.5 Results 143
- Electrode test 145
- 5.6 Sample table 146
- 5.6 Sample table 147
- Voltammogram 154
- Chronoamperogram 154
- Minimum 157
- Recommended 157
- 6 Electroplating Bath VA 162
- Calibra 205
- Calibration 205
- Calibration tech 207
- 7 Manual control 209
- 7 Manual control 210
- 7.2 Dosing Device control 211
- 7.3 Pump control 212
- 7.4 Film deposition 213
- 7.5 Cleaning procedure 215
- 8 How to ...? 217
- 8.2 User rights 218
- DOSINOS window: 239
- Suppressor standard 247
- Rinsing solution 247
- Response curve) 253
- 8.10 Diagnostic procedures 265
- 9 Troubleshooting 269
- 9.4 Dosing Device problems 270
- 9 Troubleshooting 272
- AC – Alternating 273
- FICATION 273
- METHOD PARAMETERS 273
- 9.6 Voltammetric problems 274
- 9.6 Voltammetric problems 275
- Software license 288
- Software license 289
- Index 291
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